专利摘要:
A process in which a gas is first compressed by a multistage compressor (1) and then dried by a pressure modulated adsorber (50). The pressure modulated adsorber comprises a first chamber (10) containing a first adsorbent (13). This first chamber is supplied with wet gas coming from an outlet of the last stage (1c) of the compressor, and said chamber supplies dried gas to a user. The pressure swing adsorber further includes a second chamber (20) containing a second adsorbent (23) which may have previously adsorbed moisture from the gas. In order to regenerate the second adsorbent and to desorb moisture, part of said dried gas, instead of escaping into the atmosphere, is introduced into the second chamber, and the second chamber is ventilated into a gas inlet. intermediate stage (5, 5a, 5b) of the compressor, this process thus improving the overall efficiency of the process. A device for implementing this method is also provided.
公开号:BE1023605B1
申请号:E2016/5461
申请日:2016-06-22
公开日:2017-05-12
发明作者:Anthony John Kitchener
申请人:Ateliers François;
IPC主号:
专利说明:

METHOD AND APPARATUS
TO COMPRESS AND DRY A GAS
Field of the Invention The invention relates to an apparatus and method for compressing and drying a gas. The invention relates more particularly to an apparatus and a method for providing to a user a gas dried at a high pressure and at a high flow rate, such as, for example, a pressure greater than 10 bar and a flow rate greater than 1 m 3 / min and ranging from up to 100 m3 / min.
Description of the prior art
Gas compressors of many types are technically known. It is also known that a compressed gas, particularly compressed air, has a relatively high moisture content when leaving the compressor, and that such moisture content must be eliminated or at least reduced before supplying the compressed gas. to a user.
Several methods have been proposed for drying a compressed gas.
A known method is to cool the compressed gas, so that its water vapor content condenses, after which the liquid water is purged. In general, the dried gas must then be heated again to obtain a temperature which is that required for the future use of said gas. Although such dryers work well, they consume some energy and, as a result, reduce the overall efficiency of the apparatus. It is not uncommon for such a refrigerated dryer to consume from 3% to 5% of the total energy consumption of the apparatus, in particular in the case of a compressor operating at high pressure and at a high flow rate, such as a multi-stage compressor for example. Such refrigerated dryers also have many other drawbacks: they are very difficult to transport, they require a specific power supply and specific water cooling lines, they must be monitored and recharged with a refrigerant which must satisfy stringent and varying regulatory requirements in various countries, etc.
Another known method is to adsorb the water vapor of the compressed gas on a desiccant. In such desiccant dryers, however, the desiccant must be regenerated or replaced when it is saturated with moisture. Two conventional methods for regenerating a saturated desiccant are the temperature modulated adsorption (TSA) method and the pressure swing adsorption (PSA) method.
With the TSA process, the desiccant is regenerated by heating it to elevated temperatures, typically over 120 ° C, which causes desorption of previously adsorbed moisture. After this step, the desiccant must be cooled, preferably with dry cooling air, in order to be able to effectively adsorb the water vapor from the wet compressed gas again.
Such a process is for example known from US Pat. No. 622,111,30. Here, the desiccant to be regenerated is placed in the gas stream of an intermediate stage of a multistage compressor, and the heat of this gas is Intermediate stage is used to desorb previously adsorbed moisture from the compressor outlet.
Such a process has the disadvantage that it uses relatively humid air for the regeneration process, which affects the efficiency of this process. The efficiency of this process also depends on the temperature of the intermediate stage compressed gas, a parameter which generally can not be chosen freely because it depends on the compression process. In comparison with the PSA process, which will be detailed hereinafter, the TSA process is also much slower because of the time required to heat and then cool the desiccant at each regeneration cycle. As a further negative consequence of the foregoing, the TSA tanks, which contain the desiccant, must be large, and where there are large tanks that must withstand high pressure, they must have thick walls and are very expensive to use. manufacture.
A compressor using a TSA dryer is also known from European patent publication EP 799635. Here, a relatively dry gas from the compressor outlet is used for the regeneration of the saturated desiccant, once this gas has been removed. first heated using the compression heat generated by the compressor. Apart from the advantage of using a relatively dry gas for regeneration, this process suffers from the same disadvantages as the previous process.
A compressor using TSA dryer is also known from US patent application US2014 / 0190349. Here, the gas of an intermediate stage of the compressor is dried by a TSA dryer before a part of it is supplied to a next stage of the compressor. Another portion of the intermediate dried gas is used for the regeneration of the saturated desiccator of the TSA dryer after this gas has first been reheated. This device suffers the same disadvantages as the previous. It should also be noted that there is no drying of the gas produced at the outlet of the compressor, which can result in an output gas that is too wet.
The PSA process does not use temperature changes, but rather changes in pressure, to release the adsorbed moisture. Typically, a desiccant adsorbs moisture at high pressure. The process then proceeds to a lower pressure-typically atmospheric pressure-to desorb the moisture adsorbed by the desiccant. Adsorption and desorption can operate at near ambient temperature and do not need external heating or cooling, which is an advantage over the TSA process. However, the PSA process has the disadvantage that part of the compressed gas is lost during the regeneration cycle. The PSA process is furthermore technically known to be unsuitable for drying gases at high pressures and / or at high flow rates. Summary of the invention
An object of the invention is to provide a method and apparatus for compressing and drying a gas, said invention addressing the problems of the state of the processes and apparatus of the art concerned. An object of the invention is more particularly to provide a method and an apparatus for supplying a dried gas at a high pressure and at a high flow rate, for example a pressure greater than 10 bar and a flow rate greater than 1 m 3 / min. and up to 100 m3 / min. The invention is defined by the independent claims. The dependent claims define advantageous embodiments.
In accordance with the invention there is provided a method for compressing and drying a gas, said method comprising the steps of: - compressing the gas in a multistage compressor having at least three successive compressor stages, an inlet of a first stage gas, a last stage gas outlet providing a last stage compressed gas, a first intermediate stage portion operating at a first intermediate pressure, and a second intermediate stage portion operating at a second intermediate pressure which is greater than the first intermediate pressure, - drying the last stage compressed gas, by introducing it into a first chamber containing a regenerable first adsorbent, said first chamber providing, at a dried gas outlet, a dried gas intended a user - to regenerate a second regenerable adsorbent contained in a second th chamber, by introducing into said second chamber a portion of the dried gas from the dried gas outlet and by ventilating the second chamber in a gas inlet of the compressor, the method being characterized in that the ventilation step of the second chamber comprises two successive substeps: a first substep during which the second chamber is ventilated in a second intermediate stage gas inlet of the second intermediate stage part, and a second substep during wherein the second chamber is vented into a first intermediate stage gas inlet of the first intermediate stage portion.
This process is different from the refrigeration process and the TSA process and, therefore, does not reveal the aforementioned disadvantages of these methods. The process according to the invention makes use of the PSA process, but in a new and specific way, namely by regeneration ventilation sequentially in different intermediate stages of the multi-stage compressor, so that it avoids too large and / or negative pressure differences during ventilation, and so that the compressed gas used for this purpose is not wasted by discharge into the atmosphere, but is reintroduced into the compressor, which results in a better total efficiency of the device, compared to existing processes.
In a preferred method according to the invention, the first and second chambers are mutually permuted in a periodic manner, so that the step of drying the top stage compressed gas occurs during a first period of time in the first chamber, while the regeneration step of the second regenerable adsorbent occurs in the second chamber, and vice versa, during a second period of time.
Apart from the time required to switch the first and second chambers, it is possible to provide a user, almost continuously, compressed and dried gas.
More preferably, the step of compressing the gas is a step of compressing the gas at a last stage outlet pressure that is greater than 10 bar, preferably greater than 20 bar, more preferably greater than 30 bar.
In each and any of these cases, said gas is preferably air. The invention also relates to an apparatus for implementing these methods.
Brief description of the drawings
These and other aspects of the invention will be explained in more detail by way of examples and with reference to the accompanying drawings in which:
Figure 1 shows schematically an apparatus -cité by way of example - according to the invention;
Figure 2 schematically shows an example -cité by way of example - according to a preferred embodiment of the invention;
Figure 3 shows schematically the apparatus of Figure 2, when said apparatus is in a first phase of operation;
Figure 4 shows schematically the apparatus of Figure 2, when said apparatus is in a second phase of operation;
Fig. 5 schematically shows an exemplary apparatus according to a more preferred embodiment of the invention;
Figure 6 shows schematically the apparatus of Figure 5, when said apparatus is in a first phase of operation;
Figure 7 shows schematically the apparatus of Figure 5, when said apparatus is in a second phase of operation;
Figure 8 shows schematically the apparatus of Figure 5, when said apparatus is in a third phase of operation;
Figure 9 shows schematically the apparatus of Figure 5, when said apparatus is in a fourth phase of operation;
Figure 10 schematically shows an exemplary apparatus according to an even more preferred embodiment of the invention;
Fig. 11 schematically shows an exemplary apparatus according to an even more preferred embodiment of the invention;
Figure 12 schematically shows a portion of an exemplary apparatus - in accordance with a preferred embodiment of the invention.
The drawings of the figures are neither drawn to scale nor proportioned. In general, similar or identical components are indicated by the same reference numerals in the figures.
DETAILED DESCRIPTION OF EMBODIMENTS OF THE INVENTION
Figure 1 schematically shows an exemplary apparatus according to the invention and comprising a multi-stage gas compressor (1) followed by a gas dryer or dehumidifier (50).
The multistage compressor can be any type of gas compressor. As is well known, a multistage compressor comprises intermediate stage portions between any two adjacent compression stages, these intermediate stage portions respectively operating at increasing intermediate pressures.
In the example illustrated in FIG. 1, the multistage compressor is a three-stage compressor comprising, successively, a first stage (1a) having a first stage gas inlet (4) to which gas to be compressed is supplied. said first stage being followed by a second stage (1b) followed by a third stage (1c) from which compressed gas is supplied to a last stage outlet (6). The compressor of FIG. 1 has a first intermediate stage portion (lab) placed between the first and second stages and operating at a first intermediate pressure, and a second intermediate stage portion (lbc) placed between the second and the second stage. third stage and operating at a second intermediate pressure which is greater than the first intermediate pressure. In this example, the second intermediate stage part (lbc) comprises an intermediate stage gas inlet (5) to which gas can be supplied, in addition to the gas stream coming from an upstream stage, like this will be explained below. The apparatus further comprises a dryer (50) having a first chamber (10) containing a first regenerable adsorbent (13) and having a second chamber (20) containing a second regenerable adsorbent (23). The regenerable adsorbents (13, 23) are those which are capable of adsorbing moisture from a gas, adsorbents such as zeolites or activated alumina or silica gels, for example.
As shown in Figure 1, the apparatus also includes a first valve (34) and a second valve (35), corresponding valve controls (not shown) and gas lines, all configured for, during a first period of time: - connect the first chamber (10) in series between the last stage gas outlet (6) and a dried gas outlet (40) provided for a user, and to - connect the second chamber (20) in series between said dried gas outlet (40) and at least one of at least one intermediate stage gas inlet of the multistage compressor.
In this example, the second chamber (20) is connected in series between said dried gas outlet (40) and an intermediate stage gas inlet (5) located in the second intermediate stage portion (1bc) of the compressor. several stages, but said chamber may also be connected in series between said dried gas outlet (40) and an intermediate stage gas inlet located in the first intermediate stage portion (lab) of the multistage compressor.
With such a configuration, wet gas, which is provided by the last stage (1c) of the compressor, can be dried by the first regenerable adsorbent of the first chamber (10), to provide a dried gas to a user, while a portion of said dried gas can be reintroduced into the second chamber (20) to regenerate the second regenerable adsorbent. A flow occurring at the dried gas outlet may, in this example, be regulated by the first valve (34), while a flow of dried gas reintroduced into the second chamber (20) may be regulated by the second valve (35). Typically, from 10% to 20% of the dried gas supplied from the first chamber (10) is introduced into the second chamber (20) to regenerate the second regenerable adsorbent. Specific to the invention is the fact that the gas, which is supplied by the second chamber, is not discharged into the atmosphere, or not completely, but rather is reintroduced at least partially into an intermediate stage part of the compressor .
In a process according to the invention, the following steps a), b) and c), which are performed to compress and dry a gas, consist of: a) Compressing the gas in a multi-stage compressor having at least one inlet of intermediate stage gas (5) and having a last stage gas outlet (6) providing a last stage compressed gas. b) drying the last stage compressed gas by introducing it into a first chamber (10) containing a first regenerable adsorbent (13), said first chamber providing, at a dried gas outlet (40), a dried gas intended for a user. c) regenerating a second regenerable adsorbent (23) contained in a second chamber (20) by introducing into said second chamber a portion of the dried gas from the dried gas outlet (40) and venting the second chamber into at least one one of at least one intermediate stage gas inlets (5).
It will be clear that such a method can, for example, be implemented with an apparatus as described above.
Figure 2 schematically shows an exemplary apparatus according to a preferred embodiment of the invention.
This apparatus is identical to the apparatus of Figure 1, except that its dryer (50) comprises four additional valves (30, 31, 32, 33), corresponding controls of the additional valves (not shown) and additional gas lines, as shown. The first and second valves (34, 35), the four additional valves (30, 31, 32, 33), the corresponding valve controls and the gas lines are all further configured for, during a second period of operation. time: - connect the second chamber (20) in series between the last stage gas outlet (6) and a dried gas outlet (40) provided for a user, and to - connect the first chamber (10) in series between said dried gas outlet (40) and at least one of at least one intermediate stage gas inlet (5) of the multi-stage compressor.
Such a dryer (5) is sometimes referred to as a pressure swing adsorption (PSA) dryer and is technically well known, for example from US Patent Publication No. 2944627 to Skarstrom, which publication is incorporated herein by reference.
As shown in Fig. 2 and the following figures, the dryer (50) has a wet gas inlet (50a), a dried gas outlet (50b) and a purge outlet (50c). The dryer (50) is controlled to operate as shown in more detail in Figure 3 and Figure 4.
Figure 3 shows schematically the apparatus of Figure 2 when said apparatus is in a first phase of operation during the first period of time. During this first phase of operation, the valve controls at least partially open the valves 30, 33, 34 and 35 and close the valves 31 and 32. As a result, wet gas, which is supplied by the last stage (the ) of the compressor, can be dried by the first regenerable adsorbent (13) of the first chamber (10), to provide a user with a dried gas (40), while a portion of said dried gas can be reintroduced into the second chamber (20) for regenerating the second regenerable adsorbent (23). Specific to the invention is the fact that the gas, which is supplied by the second chamber (20) during said first phase of operation, is not discharged into the atmosphere, or not completely, but rather is reintroduced at least partially in an intermediate stage part (5) of the compressor.
Figure 4 schematically shows the apparatus of Figure 2 when said apparatus is in a second phase of operation during the second period of time. During this second phase of operation, the valve controls at least partially open the valves 31, 32, 34 and 35 and close the valves 30 and 33. Accordingly, wet gas, which is supplied by the last stage (the ) of the compressor, can be dried by the second regenerable adsorbent (23) of the second chamber (20), to provide a user with a dried gas (40), while a portion of said dried gas can be reintroduced into the first chamber (10), for regenerating the first regenerable adsorbent (13). Specific to the invention is the fact that the gas, which is supplied by the first chamber during the second phase of operation, is not discharged into the atmosphere, or not completely, but rather reintroduced at least partially into a intermediate stage part (5) of the compressor.
The valve controls may be configured to periodically switch the apparatus between the first and second phases of operation, thereby providing an almost continuous supply of dried compressed gas to the user at the dried gas outlet (40). .
In a preferred method according to the invention, the first chamber (10) and the second chamber (20) are mutually permuted periodically, so that the step of drying the last stage compressed gas occurs in the first chamber during a first period of time, while the regeneration step of the second regenerable adsorbent occurs in the second chamber, and vice versa, during a second period of time.
Figure 5 schematically shows an exemplary apparatus according to a more preferred embodiment of the invention. This apparatus is identical to the apparatus of FIG. 2, except that it further comprises two ventilation valves (36, 37), corresponding controls of the ventilation valves (not shown) and ventilation gases, all of which are configured for, during the first period of time: - connecting the second chamber (20) in series between said dried gas outlet (40) and a second intermediate stage gas inlet (5b ) of the second intermediate stage part (lbc) during a third period of time, and for connecting the second chamber (20) in series between said dried gas outlet (40) and a first gas inlet of intermediate stage (5a) of the first intermediate stage part (lab) during a fourth period of time following the third period of time.
Ventilating the second chamber firstly in the second intermediate stage portion (lbc) rather than in the first intermediate stage portion (lab) of the multi-stage compressor, in fact has the advantage of reducing the gas flow through the second chamber during this phase of operation, which reduces the risk of entrainment of adsorbent dust and / or damage to the adsorbent, and which also reduces noise. This process also facilitates recompression by the compressor of the vented gas, which reduces energy losses and therefore increases overall efficiency.
Figure 6 shows schematically the apparatus of Figure 5 when it is in a first phase of operation during the first period of time.
During this first phase of operation, the valve controls at least partially open the valves 30, 33, 34, 35 and 37 and close the valves 31, 32 and 36 during the third period of time. As a result, the gas, which is supplied by the second chamber (20) during said first phase of operation, is reintroduced at least partially into the second intermediate stage part (lbc) of the compressor, via the second input of intermediate stage gas (5b). Accordingly, wet gas, which is provided by the last stage (1c) of the compressor, can be dried by the first regenerable adsorbent (13) of the first chamber (10), to provide a user with a dried gas, while a portion of said dried gas may be reintroduced into the second chamber (20) to regenerate the second regenerable adsorbent (23). Therefore, the gas, which is supplied by the second chamber during said first phase of operation, is reintroduced at least partially into the second intermediate stage portion (lbc) of the compressor, via the second stage gas inlet intermediate (5b).
Figure 7 shows schematically the apparatus of Figure 5 when it is in a second phase of operation during the first period of time.
During this second phase of operation, the valve controls at least partially open (or leave open) the valves 30, 33, 34, 35 and 36 and close (or leave closed) the valves 31, 32 and 37 during the fourth period of time. Accordingly, the gas, which is supplied by the second chamber during said second phase of operation, is reintroduced at least partially into the first intermediate stage part (lab) of the compressor, via the first stage gas inlet intermediate (5a).
Figure 8 shows schematically the apparatus of Figure 5 when it is in a third phase of operation during the second period of time.
During this third phase of operation, the valve controls at least partially open the valves 31, 32, 34, 35 and 37 and close the valves 30, 33 and 36 during a fifth period of time. Accordingly, the gas, which is supplied by the first chamber (10) during said third phase of operation, is reintroduced at least partially into the second intermediate stage portion (lbc) of the compressor, via the second gas inlet intermediate stage (5b).
Figure 9 shows schematically the apparatus of Figure 5 when it is in a fourth phase of operation during the second period of time.
During this fourth phase of operation, the valve controls open at least partially (or leave open) the valves 31, 32, 34, 35 and 36, and close (or leave closed) the valves 30, 33 and 37 during a sixth period of time following the fifth period of time. As a result, the gas, which is supplied by the first chamber (10) during said fourth phase of operation, is reintroduced at least partially into the first intermediate stage part (lab) of the compressor, via the first gas inlet intermediate stage (5a).
In a preferred method according to the invention, the ventilation step of the second chamber (20) comprises two successive sub-steps: a first substep during which the second chamber (20) is ventilated in one either of a first intermediate stage gas inlet (5a) of the first intermediate stage part (lab) or a second intermediate stage gas inlet (5b) of the second part of intermediate stage (lbc), and a second substep during which the second chamber (20) is respectively ventilated in one or the other of the second intermediate stage gas inlet (5b) of the second part intermediate stage (1cc) or the first intermediate stage gas inlet (5a) of the first intermediate stage part (lab).
More preferably, the second chamber (20) is vented into the second intermediate stage gas inlet (5b) of the second intermediate stage portion (lbc) during the first substep, and the second chamber (20) is vented in the first intermediate stage gas inlet (5a) of the first intermediate stage portion (lab) during the second substep, said second substep occurring after the first sub-stage step.
Preferably, the step of ventilating the first chamber (10) occurring during the second period of time also comprises two successive substeps, namely a third sub-step during which the first chamber (10) is vented into the second intermediate stage gas inlet (5b) of the second intermediate stage portion (lbc), and a fourth sub-stage during which the first chamber (10) is vented into the first inlet of intermediate stage gas (5a) of the first intermediate stage part (lab), said fourth substep occurring after the third substep.
As stated above, typically from 10% to 20% of the dried gas supplied by the first chamber (10) is introduced into the second chamber (20) to regenerate the second regenerable adsorbent during the first period of time (such as illustrated in Figures 3, 6, 7) and, conversely, typically 10% to 20% of the dried gas supplied by the second chamber (20) is introduced into the first chamber (10) to regenerate the first regenerable adsorbent during the second period of time (as illustrated in Figures 4, 8, 9). Accordingly, the first and second valves (34, 35) are configured and optionally controlled to achieve these flow rates. Nevertheless, the apparatus further comprises, preferably, a first bypass valve (34b) which is fluidly connected in parallel to the first valve (34), and a second bypass valve (35b) which is fluidly connected, in parallel with the second valve (35), as shown in Fig. 10. The first bypass valve (34b) is configured and optionally controlled to bypass the first valve (34) during the first period of time, and the second bypass valve (35b) is configured and possibly controlled to bypass the second valve (35) during the second period of time, so that a sufficient amount of dried gas intended for the user can be provided at the the dried gas outlet (40) during each of the first and second periods of time.
In the case where the first and second bypass valves (34b, 35b) are control valves, a controller opens the first bypass valve (34b) and closes the second bypass valve (35b) during the first period of time , and the regulator closes the first bypass valve (34b) and opens the second bypass valve (35b) during the second period of time.
Alternatively, the first and second bypass valves (34b, 35b) may be one-way valves (also known as non-return valves), each of which is so oriented that gas can flow to through these bypass valves, respectively from the first and second chambers (10, 20) to the dried gas outlet (40), and not in the opposite direction. An exemplary embodiment is schematically shown in Figure 11, where gas flow directions in one direction through one-way valves are indicated by arrows.
Preferably, the first and second bypass valves are one-way, spring loaded valves.
Preferably, the step of compressing the gas is a step of compressing the gas at a last stage outlet pressure (6) which is greater than 10 bar, preferably greater than 20 bar, more preferably greater than 30 bar. bars.
Therefore, the multistage compressor of an apparatus according to the invention is preferably adapted to compress gas at a last stage outlet pressure which is greater than 10 bar, preferably greater than 20 bar, more preferably better than 30 bars.
Preferably, said gas is air, more preferably ambient air.
Preferably, the first regenerable adsorbent (13) is fixed on a surface of a first rigid structure (15a), said first rigid structure being fixed inside the first chamber (10) and on the latter, the second regenerable adsorbent (23) being fixed on a surface of a second rigid structure (15b), said second rigid structure being attached to and within the second chamber (20). Contrary to the known use of adsorbent-coated granules or grains in the PSA dryer chambers, the inventor has found that such a rigid structure (15) is more suitable for treating compressed gases in a PSA dryer. at high pressures (pressures such as those above 10 bar) and / or high gas flow rates (flow rates such as those greater than 1 m3 / min and up to 100 m3 / min for example).
More preferably, each of the first (15a) and second (15b) rigid structures is a channelized honeycomb structure. FIG. 12 schematically shows a chamber, mentioned by way of example, which may be one or the other of the first chamber (10) and / or the second chamber (20) and comprising a canalized structure in a nest bee (15a, 15b) which is arranged axially inside the chamber and fixed thereto rigidly. The chamber also has gas inlet and outlet ports, as indicated by arrows in Figure 10. Preferably, the inlet and outlet ports are axially arranged.
The rigid structure, itself, can be composed for example of fiberglass reinforced cardboard or any other suitable rigid material.
Each channel of the honeycomb structure is, for example, embedded or impregnated, inside said channel and along its length, with a regenerable adsorbent (13, 23) such as silica gel or zeolites or activated alumina.
With such rigid structures, the inventors have found that gas velocities inside the chambers (10, 20), up to 3/10 m / s or even up to 5 m / s, can be used without major disadvantages. These speeds are 5 to 10 times higher than those obtained by using chambers filled with adsorbent-coated granules, thus making it possible to remove even more than 90% of the moisture contained in the incoming gas.
In a more preferred embodiment of the apparatus, the first and second chambers (10, 20) are elongated chambers both of which are arranged horizontally. Preferably, the gas flow in the first and second chambers is a substantially horizontal gas flow.
The present invention has been described in terms of specific embodiments which illustrate the invention and should not be construed as limiting. More generally, the technically expert persons will know that the present invention is not limited by what has been in particular shown and / or described above.
The reference numerals in the claims do not limit the extent of their protection. The use of the verbs "to understand", "to contain", "to be composed of", or of any other variant, as well as of their respective conjugations, does not exclude the presence of elements other than those stated. The use of the article "a", "a" or "the", "the" preceding an element does not exclude the presence of a plurality of such elements.
A process according to the invention can also be described as follows: a process in which a gas is first compressed by a multi-stage compressor (1) and then dried by a pressure-modulating adsorber (50). The pressure modulated adsorber comprises a first chamber (10) containing a first adsorbent (13). This first chamber is fed with wet gas from an outlet of the last stage (1c) of the compressor, and said chamber supplies dried gas to a user. The pressure modulated adsorber further comprises a second chamber (20) containing a second adsorbent (23) which may have previously adsorbed moisture. In order to regenerate the second adsorbent and desorb the moisture, a portion of said dried gas is introduced into the second chamber, and the second chamber is sequentially ventilated in at least two different intermediate stage gas inputs (5b, 5a) of the compressor instead of escaping into the atmosphere, which reduces pressure differences during ventilation and improves the overall efficiency of the process.
权利要求:
Claims (10)
[1]
CLAIMS (amended)
A method for compressing and drying a gas, comprising the steps of: - compressing the gas in a multi-stage compressor (1) having at least three successive compressor stages (1a, 1b, 1c), a gas inlet of first stage (4), a last stage gas outlet (6) providing a last stage compressed gas, a first intermediate stage part (lab) operating at a first intermediate pressure, and a second intermediate stage part ( lbc) operating at a second intermediate pressure which is greater than the first intermediate pressure; - drying the last stage compressed gas by introducing it into a first chamber (10) containing a first regenerable adsorbent (13), said first chamber providing, at a dried gas outlet (40), a dried gas intended for a user; - regenerating a second regenerable adsorbent contained in a second chamber (20), introducing into said second chamber a portion of the dried gas from the dried gas outlet (40) and venting the second chamber into a compressor gas inlet, characterized in that the step of venting the second chamber (20) comprises two successive sub-steps: a first substep during which the second chamber (20) is ventilated in a second intermediate stage gas inlet (5b) of the second intermediate stage part (lbc), and a second substep during which the second chamber (20) is vented into a first intermediate stage gas inlet (5a) of the first intermediate stage part (lab).
[2]
2. Method according to claim 1, characterized in that the first and second chambers (10, 20) are mutually permuted in a periodic manner, so that the step of drying the last stage compressed gas occurs in the first stage. chamber (10) during a first period of time, while the regeneration step of the second regenerable adsorbent (23) occurs in the second chamber (20), and vice versa, during a second period of time. time.
[3]
3. Method according to any one of the preceding claims, characterized in that the step of compressing the gas is a step of compressing the gas at a last stage outlet pressure which is greater than 10 bar, preferably greater than 10 bar. 20 bars, more preferably greater than 30 bars.
[4]
An apparatus for compressing and drying a gas, said apparatus comprising: - a multistage compressor (1) having at least three successive compressor stages (1a, 1b, 1c), a first stage gas inlet (4), a last stage gas outlet (6) for supplying a last stage compressed gas, a first intermediate stage part (lab) operating at a first intermediate pressure, and a second intermediate stage part (lbc) operating at a first stage stage second intermediate pressure which is greater than the first intermediate pressure; - a dryer (50) comprising a first chamber (10) containing a first regenerable adsorbent (13), and comprising a second chamber (20) containing a second regenerable adsorbent (23) a first valve (34) and a second valve (35), corresponding controls of the valves and gas lines, all these elements being configured for, during a first period of time; emps: - connect the first chamber (10) in series between the last stage gas outlet (6) and a dried gas outlet (40) provided for a user, and for - connect the second chamber (20) in series between said dried gas outlet (40) and a multi-stage compressor gas inlet, characterized in that the apparatus further comprises two ventilation valves (36, 37), corresponding controls of the ventilation valves and ventilation gas, all configured for, during the first period of time, connecting the second chamber (20) in series between said dried gas outlet (40) and a second intermediate stage gas inlet (5b) of the second intermediate stage portion (lbc) during a third period of time, and for connecting the second chamber (20) in series between said dried gas outlet (40) and a first intermediate stage gas inlet ( 5a) of the first part of intermediate age (lab) during a fourth period of time following the third period of time.
[5]
5. Apparatus according to claim 4, characterized in that it further comprises four additional valves (30, 31, 32, 33), and in that the first valve (34), the second valve (35), the four additional valves (30, 31, 32, 33), the two ventilation valves (36, 37), the corresponding valve controls and the gas lines, are all further configured for, during a second period of time : - connect the second chamber (20) in series between the last stage gas outlet (6) and the dried gas outlet (40), and to - connect the first chamber (10) in series between the dried gas outlet (40) the second intermediate stage gas inlet (5b) of the second intermediate stage part (Ibc) during a fifth period of time, and for - connecting the first chamber (10) in series between said dried gas outlet (40) and the first intermediate stage gas inlet (5a) of the first stage portion in intermediate (lab) during a sixth period of time following the fifth period of time.
[6]
6. Apparatus according to any one of claims 4 to 5, characterized in that it further comprises a first bypass valve (34b) fluidically connected in parallel with the first valve (34), and a second bypass valve ( 35b) fluidically connected in parallel with the second valve (35).
[7]
7. Apparatus according to claim 6, characterized in that the first and second bypass valves (34b, 35b) are single-way valves, each of these valves being oriented in such a way that air can flow. respectively from the first and second chambers (10, 20) to the dried gas outlet (40).
[8]
Apparatus according to one of claims 4 to 7, characterized in that the multi-stage compressor (1) is adapted to compress the gas at a last stage gas outlet pressure (6) which is greater than 10 bars, preferably greater than 20 bar, more preferably greater than 30 bar.
[9]
9. Apparatus according to any one of claims 4 to 8, characterized in that the first regenerable adsorbent (13) is fixed on a surface of a first rigid structure (15a), said first rigid structure being fixed inside. of the first chamber (10) and thereabove, and in that the second regenerable adsorbent (23) is fixed on a surface of a second rigid structure (15b), said second rigid structure being fixed inside the the second chamber (20) and on it.
[10]
10. Apparatus according to claim 9, characterized in that each of the first and second rigid structures is a channelized honeycomb structure.
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同族专利:
公开号 | 公开日
KR20180042222A|2018-04-25|
WO2016207237A1|2016-12-29|
BE1023605A1|2017-05-12|
RU2018101700A|2019-07-25|
US20180185780A1|2018-07-05|
AU2016282331A1|2018-02-08|
MX2017016903A|2018-08-15|
EP3954454A1|2022-02-16|
US10464010B2|2019-11-05|
EP3108953A1|2016-12-28|
CN107921359A|2018-04-17|
CA2990419A1|2016-12-29|
CN107921359B|2021-02-09|
引用文献:
公开号 | 申请日 | 公开日 | 申请人 | 专利标题
EP0799635A1|1996-04-02|1997-10-08|Atlas Copco Airpower N.V.|Method and device for drying a compressed gas|
US7250150B1|1999-06-10|2007-07-31|Questair Technology, Inc.|Chemical reactor with pressure swing adsorption|
US20050199124A1|2004-03-12|2005-09-15|Little William A.|Device and method for removing water and carbon dioxide from a gas mixture using pressure swing adsorption|
US20140190349A1|2013-01-10|2014-07-10|Mitsubishi Heavy Industries, Ltd.|Dehydration equipment, gas compression system, and dehydration method|
US2944627A|1958-02-12|1960-07-12|Exxon Research Engineering Co|Method and apparatus for fractionating gaseous mixtures by adsorption|
DE3271266D1|1981-11-18|1986-06-26|Duphar Int Res|Arylphenyl ethers having herbicidal activity|
US6171377B1|1999-07-14|2001-01-09|Henderson Engineering Co., Inc.|Regenerative compressed air/gas dryer|
US6221130B1|1999-08-09|2001-04-24|Cooper Turbocompressor, Inc.|Method of compressing and drying a gas and apparatus for use therein|
CN2573059Y|2002-10-16|2003-09-17|席玉明|Compression heat adsorbing drying machine|
BE1016309A3|2004-11-10|2006-07-04|Atlas Copco Airpower Nv|METHOD FOR DRYING COMPRESSED GAS AND APPARATUS APPLIED THEREOF|
BE1017776A3|2007-10-04|2009-06-02|Atlas Copco Airpower Nv|METHOD FOR DRYING COMPRESSED GAS|
BE1018590A3|2009-10-30|2011-04-05|Atlas Copco Airpower Nv|DEVICE FOR COMPRESSING AND DRYING GAS AND A METHOD THEREOF|
US8951339B2|2011-10-21|2015-02-10|Henderson Engineering Company, Inc.|Compressed gas drying system|
EP2724770A1|2012-10-26|2014-04-30|Alstom Technology Ltd|Absorption unit for drying flue gas|
US9186623B2|2013-03-13|2015-11-17|Roger's Machinery Company, Inc.|Recycled purge air dryer system and method of use|
CN104059692B|2014-05-23|2016-03-30|四川天采科技有限责任公司|A kind of method combining recover hydrogen, carbon two and above cut lighter hydrocarbons|
BE1024396B1|2016-10-25|2018-02-13|Atlas Copco Airpower Naamloze Vennootschap|Compressor installation with drying device for compressed gas and method for drying compressed gas.|NL2025046B1|2020-03-04|2021-10-14|Valentin Peter|Method and device for controlling several compressors connected to a compressed air installation|
法律状态:
优先权:
申请号 | 申请日 | 专利标题
EP15173873.9A|EP3108953A1|2015-06-25|2015-06-25|Method and apparatus for compressing and drying a gas|
EP15173873.9|2015-06-25|
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